مشخصات پژوهش

صفحه نخست /Preparation and ...
عنوان Preparation and characterization of nano-Co-[4-chlorophenyl-salicylaldimine-methyl pyranopyrazole]Cl-2 as a new Schiff base complex and catalyst for the solvent-free synthesis of 1-amidoalkyl-2-naphthols
نوع پژوهش مقاله چاپ‌شده
کلیدواژه‌ها 1-amidoalkyl-2-naphthol; nano-[co-4CSMP]Cl-2; pyranopyrazole; Schiff base
چکیده y the reaction of 4-chlorobenzaldehyde with ethyl acetoacetate, malononitrile, and hydrazine hydrate, 6-amino-4-(4-chlorophenyl)-3-methyl-2,4-dihydropyrano[2,3-c]pyrazole-5-carbonitrile was prepared and then reacted with salicylaldehyde and CoCl2 center dot 6H(2)O to produce nano-Co-[4-cholorophenyl-salicylaldimine-methylpyranopyrazole]Cl-2 (nano-[Co-4CSMP]Cl-2). The prepared nano-Schiff base complex was reported for the first time and fully characterized by Fourier transform-infrared spectroscopy, thermal gravimetric analysis, differential thermal gravimetric analysis, scanning electron microscopy, energy-dispersive X-ray spectroscopy, transmission electron microscopy, and Brunner-Emmett-Teller analyses and applied as an efficient catalyst for the synthesis of some 1-amidoalkyl-2-naphthol derivatives.
پژوهشگران فاطمه نورایی (نفر سوم)، حمید گودرزی افشار (نفر دوم)، احمد رضا موسوی زارع (نفر اول)